An investigation on the influence of sintering temperature on microstructural, physical and mechanical properties of cu-sic composites

Somani, N; Tyagi, Y K and Gupta, N K (2024) An investigation on the influence of sintering temperature on microstructural, physical and mechanical properties of cu-sic composites. Journal of Engineering, Design and Technology, 22(1), pp. 77-88. ISSN 1726-0531

Abstract

Purpose: The purpose of this study is to investigate the effect of the sintering temperature on the microstructural, mechanical and physical properties of Cu-SiC composites. Design/methodology/approach: The powder metallurgy route was used to fabricate the samples. Cold compaction of powders was conducted at 250 MPa which was followed by sintering at 850°C–950°C at the interval of 50 °C in the open atmospheric furnace. SiC was used as a reinforcement and the volumetric fraction of the SiC was varied as 10%, 15% and 20%. The processed samples were metallurgically characterized by the scanning electron microscope (SEM). Mechanical characterization was done using tensile and Vickers' micro-hardness testing to check the hardness and strength of the samples. Archimedes principle and Four-point collinear probe method were used to measure the density and electrical resistivity of the samples. Findings: SEM micrograph reveals the uniform dispersion of the SiC particles in the Cu matrix element. The results revealed that the Hardness and tensile strength were improved due to the addition of SiC and were maximum for the samples sintered at 950 °C. The addition of SiC has also increased the electrical resistivity of the Cu-SiC composite and was lowest for Cu 100% while the relative density has shown the reverse trend. Further, it was found that the maximum hardness of 91.67 Hv and ultimate tensile strength of 312.93 MPa were found for Cu-20% SiC composite and the lowest electrical resistivity of 2.017 µ- Ω-cm was found for pure Cu sample sintered at 950 °C, and this temperature was concluded as the optimum sintering temperature. Research limitations/implications: The powder metallurgy route for the fabrication of the composites is a challenging task as the trapping of oxygen cannot be controlled during the compaction process as well as during the sintering process. So, a more intensive study is required to overcome these kinds of limitations. Originality/value: As of the author’s best knowledge, no work has been reported on the effect of sintering temperature on the properties of the Cu-SiC composites which has huge potential in the industries.

Item Type: Article
Uncontrolled Keywords: cu-sic composite; electrical conductivity; hardness; powder metallurgy; sintering temperature; ultimate tensile strength
Index terms: mechanical property, tensile strength, methodology, furnace, conductivity, scanning electron microscope, relative density, composite, density, fabrication, testing, investigation, physical property, reinforcement
Subjects: materials science, data collection methods, mechanical systems, professional practice, analytical methods, building materials, material properties and characteristics, manufacturing engineering, research methods
Topics: Urban Studies, Engineering Principles, Construction Materials, Research Practice
Descriptive scope: 4 PCTA

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